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Effects of Ionic Liquids on the Catalytic Properties of Prussian Blue Analogues

Ying Shen  Jian Fang  Jihua Zhao  Weiguo Shen  
【摘要】:Researches on the performance of Co(Ⅱ)Fe(Ⅲ)Prussian blue analogue(Co(Ⅱ)Fe(Ⅲ)PBA) modified with several ionic liquids and the effects on the catalytic performance in the epoxidation of the styrene had been studied.The results indicated that the Co(Ⅱ)Fe(Ⅲ)PBA catalyst modified with 1-butyl-3-methylimidazolium bis(trifluoromethylsulfonyl)-imide([BMIM]TF_2N) showed the best catalytic efficiency,so we conducted the properties of various PBAs with [BMIM]TF_2N in the following step.To explore their structures,a series techniques including infrared spectroscopy(IR),X-ray diffraction(XRD),scanning electron microscopy(SEM),X-ray photoelectron spectroscopy(XPS),N_2 adsorption/desorption,NH_3-TPD measurement had been applied.It is found that the strength of lewis acid and the valence state of the Fe in the catalyst play an important role in the catalytic reaction and these gives a guidance function to our future research.

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