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A closed sample cell and co-used furnace designed for micro-Raman spectra study on volatile melts

【摘要】:正There are some difficulties in sample cell design for Raman spectrum measurements of the high-temperature volatile melts,especially the molten fluoride or chloride which is strongly corrosive. Generally,the cell should meet the requirement of anti-corrosive and anti-heat attack,and the thermal gradients of the cell should be low enough to ensure the temperature measurement accuracy.In the present study,a closed cell idea for micro-Raman spectrum measurement of volatile liquid is proposed.The sample cell and furnace is described in details.Raman spectra of various volatile liquids obtained by using

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