Synthesis and Crystal Structure of 4-Bromo-2-{(E)-3-[1-(hydroxyimino)-ethyl]phenyliminomethyl}phenol
【摘要】：正A new compound 4-Bromo-2-{(E)-3-[1-(hydroxyimino)-ethyl]phenyliminomethyl}phenol has been synthesized and structurally characterized by single-crystal X-ray diffraction.In the title compound, C_(15)H_(13)BrN_2O_2,the oxime unit adopts an E conformation with respect to the O-H group.A classical intramolecular O-H…N hydrogen bond results in the formation of a six-membered ring.The crystal structure is stabilized by intermolecular O-H…N hydrogen bonds between the hydroxy groups and the oxime N atoms.In addition,the crystal structure also features short intermolecular Br…Br short contacts with a distance of 3.8768(5)A.
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